Scanning Transmission X-ray Microscope (STXM)

Characteristics

Energy range

200-1900 eV

Monochromator

Variable-included-angle PGM, Calculated Flux ~1012 photons/s, Resolving Power (1.9 GeV, 400 mA) E/DE 2500–7500

Characteristics

Used to make x-ray images and NEXAFS spectra of thin samples in transmission
Spatial Resolution
Scanning microscope with focusing by means of Fresnel zone plates; resolution determined by spot size, which is 40 nm with current zone plates but will improve with new zone plates.
Spot size at sample
40 nm with current zone plates
Samples

Thin sections or films (100 nm thick), 3 x 3 mm in area

Sample Environment
Helium at 1 atmosphere
Special Notes
Samples may be wet or dirty: thin films may be deposited on silicon nitride windows; optical alignment is provided by looking at the back side of the sample to locate regions of interest from optical micrographs
Scientific Applications
Molecular environmental science, polymer studies, studies of biofilms
Experimental Techniques
Imaging, NEXAFS in small spots